The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jan. 23, 1979

Filed:

Aug. 19, 1977
Applicant:
Inventors:

Donald E Smith, Tallmadge, OH (US);

Charles B Jones, Akron, OH (US);

Assignee:
Attorney:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
C07C / ; C07C / ;
U.S. Cl.
CPC ...
260578 ; 260582 ; 260608 ; 2606 / ; 260705 ;
Abstract

Method of preparing 2,2'-dithiodianiline by the steps of (A) obtaining an agitated mixture of a water solution of a salt of o-aminothiophenol and an unstable dispersion therein of a liquid hydrocarbon, (B) oxidizing said salt by the slow addition of a water soluble peroxide, (C) discontinuing the agitation to allow the formation of a sharply defined lower aqueous phase and upper hydrocarbon phase, (D) drawing off said lower aqueous phase and (E) distilling the hydrocarbon phase therefrom and recovering said 2,2'-dithiodianiline as a distilland.


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