The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Oct. 10, 1978

Filed:

Sep. 14, 1977
Applicant:
Inventors:

William Shepherd Hollingshead, Cuyahoga Falls, OH (US);

Edward Norbert Nowak, Uniontown, OH (US);

Assignee:
Attorney:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
C07C / ;
U.S. Cl.
CPC ...
568768 ; 568753 ;
Abstract

Hydroquinone having a purity greater than 99 percent is isolated through an aqueous recovery scheme compatible with the methyl isobutyl ketone based diisopropylbenzene dihydroperoxide isolation process. Hydroquinone, from the Hock-splitting reaction, is extracted into water while the impurities are concentrated in a distillation tower. Phase separation of the distillation tower bottoms affords an efficient separation of the hydroquinone from the organic impurities. Concentration, crystallization, and solid liquid separation (centrifugation) of the aqueous phase yields a wet hydroquinone cake which, upon recrystallization from acetone, yields high purity hydroquinone.


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