The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jul. 25, 1978

Filed:

Oct. 12, 1976
Applicant:
Inventor:

Jerry L Price, Texas City, TX (US);

Assignee:

Monsanto Company, St. Louis, MO (US);

Attorneys:
Primary Examiner:
Int. Cl.
CPC ...
C07C / ; C07C / ; C07C / ; C07C / ;
U.S. Cl.
CPC ...
260532 ; 260410 ; 2604 / ; 260413 ; 260419 ; 2605 / ; 2605 / ; 2605 / ; 260525 ; 2605 / ; 2605 / ; 260540 ; 260541 ; 560 78 ; 560 79 ; 560 97 ; 560105 ; 560109 ; 560114 ; 560191 ; 560204 ; 560232 ; 560233 ;
Abstract

A method is provided for the removal of contaminating alkanes from the vaporized carbonylation products of a process wherein carboxylic acids are produced by the reaction in the liquid phase of an alcohol or an ester, halide or ether derivative of said alcohol with carbon monoxide in the presence of a catalyst system containing a rhodium or iridium component and an iodine or bromine component. The method involves distillation of the alkane-containing vaporized carbonylation products, phase separation of the overhead from said distillation, further distillation of a slipstream of the resulting heavy phase using carbon monoxide as stripping gas and removal of the alkanes as the bottoms stream from the latter distillation.


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