The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Apr. 04, 1978

Filed:

Aug. 18, 1976
Applicant:
Inventors:

Norman A Portnoy, Hopatcong, NJ (US);

David Paul Anderson, Amherst, MA (US);

Attorneys:
Primary Examiner:
Int. Cl.
CPC ...
B01D / ; C08B / ; C08B / ;
U.S. Cl.
CPC ...
203 28 ; 203 29 ; 203 36 ; 203 37 ; 203 38 ; 203 80 ; 106168 ; 106311 ; 2605 / ; 2606 / ; 423400 ; 536 38 ;
Abstract

Recovery of the chemical components of a cellulosic organic solvent regenerating solution containing a dialkylacylamide, a lower aliphatic monohydric alcohol, a nitrite of the alcohol and nitric acid. The process comprises distilling the solution to remove the alcohol nitrite and alcohol, leaving the dialkylacylamide and nitric acid, recovering the alcohol, hydrolyzing to convert the alcohol nitrite to the alcohol and nitrous acid, neutralizing the nitric and nitrous acid with an alkali or alkaline earth metal oxide or hydroxide and distilling the solution to remove water and to separate and recover the remaining alcohol, the dialkylacylamide and the nitrate and nitrite salts. The nitrite and nitrate salts are converted by pyrolysis to nitrogen dioxide. The process results in substantially total recovery of the process chemicals.


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