The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.
The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.
Patent No.:
Date of Patent:
Feb. 07, 1978
Filed:
Nov. 03, 1976
Vincent Gerard Grosso, Piscataway, NJ (US);
American Cyanamid Company, Stamford, CT (US);
Abstract
A process for preparing a sterically hindered 3,5-dialkyl-4-hydroxybenzoic acid which comprises reacting a sterically hindered 2,6-dialkylphenol with an excess of sodium hydride or lithium hydride in a dry dipolar aprotic solvent, carboxylating the resulting anhydrous phenolate with an excess of carbon dioxide at atmospheric pressure and at a temperature of about 70.degree. C. to 80.degree. C., then destroying the excess sodium hydride or lithium hydride by addition of an alcohol, followed by acidifying the reaction mixture to obtain a high yield of the sterically hindered 3,5-dialkyl-4-hydroxybenzoic acid.
Data source: USPTO (United States Patent and Trademark Office) public patent records. Weekly synchronization. How IDiyas builds this profile