The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jan. 10, 1978

Filed:

Jul. 08, 1976
Applicant:
Inventors:

Ralph Eric Worthington, Blackrock, EI;

Padraic Seamus O'Neill, Dublin, EI;

Assignee:

Fitzwilton Limited, Dublin, EI;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C01B / ;
U.S. Cl.
CPC ...
423484 ; 423185 ; 423339 ; 423341 ; 423356 ; 423312 ; 423472 ; 423490 ; 423551 ;
Abstract

Potassium fluoride and silica are reacted with an aqueous solution of hydrofluorosilicic acid. The resulting potassium fluorosilicate is recovered. The potassium fluorosilicate may be further reacted with ammonia in water to form an aqueous mixture of ammonium fluoride and potassium fluoride. The ammonium fluoride is then heated in aqueous solution in the presence of excess potassium fluoride to release ammonia and to form potassium bifluoride. The potassium bifluoride is recovered from solution substantially free from ammonia and heated to release hydrogen fluoride. Alternatively, the recovered potassium bifluoride may be reacted with sodium fluoride to produce sodium bifluoride. The sodium bifluoride is then heated to release hydrogen fluoride.


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