The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Nov. 01, 1977

Filed:

Oct. 20, 1975
Applicant:
Inventors:

Joseph M Fox, III, Lafayette, CA (US);

Bruce D Degen, Bolinas, CA (US);

Irving Leibson, Alamo, CA (US);

Assignee:

Bechtel International Corporation, San Francisco, CA (US);

Attorney:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
C01F / ;
U.S. Cl.
CPC ...
423178 ; 423179 ; 423208 ; 423497 ;
Abstract

Carnallite, comprising principally of MgCl.sub.2. KCl.6H.sub.2 O, with varying amounts of sodium chloride and other impurities, is dissolved in a lower saturated monohydric aliphatic alcohol having from one to four carbon atoms such as methanol, ethanol, propanol, isopropyl alcohol, N-butyl alcohol, secondary-butyl alcohol, iso-butyl alcohol, and tert-butyl alcohol, to dissolve the magnesium chloride therein leaving an insoluble residue of principally potassium chloride, sodium chloride and other materials. The residue is filtered from the solution, dried and stored or further processed. The filtrate, a magnesium chloride hydrate solution is further processed by injecting steam or water into the solution and removing, e.g., evaporating the methanol from the solution leaving an aqueous magnesium chloride hexahydrate brine. The recovered methanol is dried by distillation, condensed and recycled. The brine is stored for subsequent processing or dehydrated to a magnesium chloride dihydrate and granulated for storage and subsequent use.


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