The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Oct. 11, 1977

Filed:

Nov. 01, 1976
Applicant:
Inventors:

David I Saletan, LaPorte, TX (US);

Reginald S Yeung, Houston, TX (US);

William R Pledger, Pearland, TX (US);

Assignee:

Shell Oil Company, Houston, TX (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C / ;
U.S. Cl.
CPC ...
2606 / ; 260636 ;
Abstract

Chlorohydrin reactant mixtures containing epichlorohydrin and mono- and dichlorohydrins are selectively hydrolyzed to glycerine by contact with an alkali metal carbonate catalyst, preferably sodium carbonate, at a temperature of about 50.degree. to 70.degree. C for a period of from about 20 to about 150 hours in a two phase agitated reaction system comprising an aqueous phase containing at least about 0.5% by weight alkali metal carbonate and an organic solvent phase having less than about 0.5% weight solubility in water and a dielectric constant of less than about 10, said aqueous phase being about 0.5 to about 10 times the volume of the organic solvent phase.


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