The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jun. 14, 1977

Filed:

Jul. 28, 1975
Applicant:
Inventor:

Jerry L Price, Texas City, TX (US);

Assignee:

Monsanto Company, St. Louis, MO (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
B01D / ; C07C / ;
U.S. Cl.
CPC ...
203 94 ; 203 98 ; 260941 ;
Abstract

Acetic acid containing very minor amounts of iodine, either as I.sup.-, free iodine, or alkyl iodide, or all of these, is purified by fractionation in a single column with an acid product containing 20 parts or less of iodine per billion parts of acid (ppb) being withdrawn as a liquid sidedraw from said column. Generally, more than one column is required for obtaining an acid product of such extremely high purity. The process is particularly applicable for purification of acetic acid made by the carbonylation of methanol using a catalyst system formed on the mixing of a rhodium or iridium component and an iodine component notably hydrogen iodide or an alkyl iodide such as methyl iodide.


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