The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Oct. 19, 1976

Filed:

Feb. 27, 1975
Applicant:
Inventors:

Donald H Saunders, Oreland, PA (US);

Robert A Barford, Willow Grove, PA (US);

Paul Magidman, Warrington, PA (US);

Herbert L Rothbart, Flourtown, PA (US);

Attorneys:
Primary Examiner:
Int. Cl.
CPC ...
B01D / ;
U.S. Cl.
CPC ...
2603262 ; 55386 ; 2101 / ; 210502 ; 26032631 ; 2605 / ; 260499 ; 260430 ; 252426 ; 210 / ;
Abstract

Sulfobenzylsilicas in which the organic moiety is bound to silica surfaces through a carbon-silicon bond are prepared by treating silica with thionyl chloride to chlorinate reactive silanol groups, reacting the product with benzyllithium and sulfonating the resulting benzylsilica. The sulfobenzylsilicas and their salts of noble metals are useful as bound stationary phases in various chromatographic procedures for the separation of a wide variety of natural product mixtures composed of closely related chemical compounds. For example, separation of methyl cis 9-octadecenoate and methyl trans 9-octadecenoate was readily achieved by gas-liquid chromatography on a modified silver sulfobenzylsilica column.


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