The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jun. 01, 1976

Filed:

Oct. 18, 1973
Applicant:
Inventor:

Thomas J Crossley, Chapin, SC (US);

Assignee:

Westinghouse Electric Corporation, Pittsburgh, PA (US);

Attorney:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
C01G / ; C02B / ;
U.S. Cl.
CPC ...
423-6 ; 423-7 ; 423 11 ; 423 15 ; 2523 / ;
Abstract

Waste water containing large amounts of fluorides and ammonia and trace amounts of uranium, as is produced during the hydrolysis and ammonium hydroxide treatment of uranium hexafluoride (UF.sub.6) to produce ammonium diuranate (ADU) therefrom, is rendered suitable for cyclic reuse by initially treating the waste water with sufficient lime to precipitate substantially all of the fluorides present in the waste water to a relatively insoluble CaF.sub.2 precipitate, the treated solution is subjected to distillation to drive off ammonia for reuse in the ADU precipitation, the CaF.sub.2 precipitate is separated from the aqueous distilland leaving water with dissolved calcium, the distilland is treated by a cationic ion-exchange material to remove substantially all of the calcium and other cationic metal impurities and the resulting water containing small amounts of uranium, fluoride and ammonia is recycled to react with UF.sub.6 or to be combined with the ammonium hydroxide distillate and then treated with additional concentrated ammonium hydroxide to form a solution of the desired NH.sub.3 content for use in precipitating ADU. This recycling is most important for ecological reasons, and for cost improvement, as well as health and safety purposes.


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