The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jan. 20, 1976

Filed:

Jun. 03, 1974
Applicant:
Inventors:

Wilson P Menashi, Lexington, MA (US);

Joseph F Wenckus, Needham, MA (US);

Roger A Castonguay, Salem, MA (US);

Assignee:

Arthur D. Little, Inc., Cambridge, MA (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
B01D / ; B01J / ; F27B / ;
U.S. Cl.
CPC ...
2325 / ; 2327 / ; 23290 ; 432262 ;
Abstract

Apparatus for the melt synthesis of inorganic compounds from elemental reactants, at least one of which is highly volatile at the temperature of the reaction. An enclosure means defining a reaction chamber and a reservoir-closure means containing the volatile elemental reactant form the reaction vessel which is sealed by a combination mechanical-liquid seal which is of a character to permit diffusion by high-pressure gas through it. Heating means are provided to effect at least three heating regimes: (I) liquefaction of a liquid sealant, (II) formation and maintenance of a molten reaction mass, and (III) heating of the volatile elemental reactant to vaporize it.


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