Calibration method for a differential scanning calorimeter

Abstract

A differential scanning calorimeter includes a temperature-controlled heat source and a sensor arrangement with sample- and reference-side pan support regions and measurement regions. Measurement region sensor(s) output a differential heat flow signal representative of a difference between heat flowing across the sample- and reference-side measurement regions and a sample- and reference-side local heater arrangement. A sample and reference pan are arranged on the sample and reference-side pan support region, respectively. A volume surrounding the pans is filled with a measuring gas. A steady state situation of a desired temperature is created, and once reached, heating power is applied to one of the pan support regions using the respective local heater arrangement. A second calibration factor is determined based on a ratio of a differential heat flow signal (U) and a differential heating power.