The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jun. 23, 2026

Filed:

Feb. 10, 2022
Applicant:

Basf SE, Ludwigshafen am Rhein, DE;

Inventors:

Torsten Mattke, Ludwigshafen am Rhein, DE;

Kai Thiele, Antwerp, BE;

Jens Ferbitz, Ludwigshafen am Rhein, DE;

Peter Van Den Abeel, Antwerp, BE;

Hans-Juergen Pallasch, Ludwigshafen am Rhein, DE;

Assignee:

BASF SE, Ludwigshafen am Rhein, DE;

Attorney:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
C01B 7/07 (2006.01); B01D 53/00 (2006.01); C01B 32/80 (2017.01); C07C 263/20 (2006.01);
U.S. Cl.
CPC ...
C01B 7/0712 (2013.01); B01D 53/002 (2013.01); C01B 7/0731 (2013.01); C01B 32/80 (2017.08); C07C 263/20 (2013.01); B01D 2256/26 (2013.01); B01D 2257/2064 (2013.01);
Abstract

A process of separating phosgene and hydrogen chloride, comprises: conveying a mixed stream containing hydrogen chloride and phosgene into a distillation column; withdrawing from the distillation column a bottom stream containing phosgene; withdrawing a top stream containing hydrogen chloride; compressing at least a portion of the top stream and at least partially condensing the compressed top stream to form a liquid stream, decompressing at least a portion of the liquid stream to form a cooled liquid stream and a cooled gas stream; and recycling the cooled liquid stream to the top of the distillation column as a reflux; the process additionally comprising temporarily introducing an absorbing solvent into the distillation column, in particular during starting-up and/or shutting-down of the process. The process allows for safe operation even when hydrogen chloride production only gradually begins or decreases, without the necessity of storing hydrogen chloride.


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