The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jun. 02, 2026

Filed:

Jul. 07, 2020
Applicant:

Rolls-royce High Temperature Composites Inc., Cypress, CA (US);

Inventors:

Sungbo Shim, Irvine, CA (US);

Robert Shinavski, Mission Viejo, CA (US);

Pathikumar Sellappan, Seal Beach, CA (US);

Attorney:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
C04B 35/78 (2006.01); C04B 41/45 (2006.01); C04B 41/50 (2006.01);
U.S. Cl.
CPC ...
C04B 35/78 (2013.01); C04B 41/4545 (2013.01); C04B 41/4558 (2013.01); C04B 41/4584 (2013.01); C04B 41/5066 (2013.01); C04B 41/5096 (2013.01); C04B 2235/616 (2013.01);
Abstract

A method of forming a barrier layer on a ceramic matrix composite (CMC) is described. The method includes forming a particulate surface layer comprising silicon particles on an outer surface of a fiber preform. The particulate surface layer is nitrided to convert the silicon particles to silicon nitride particles. After the nitriding, the fiber preform and the particulate surface layer are infiltrated with a molten material comprising silicon. Following infiltration, the molten material is cooled, thereby forming a ceramic matrix composite with a barrier layer thereon, where the barrier layer comprises silicon nitride and less than 5 vol. % free silicon. The barrier layer may also include silicon carbide and/or one or more refractory metal silicides.


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