The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Apr. 21, 2026

Filed:

Sep. 08, 2021
Applicant:

Nippon Shokubai Co., Ltd., Osaka, JP;

Inventors:

Hiroki Wada, Himeji, JP;

Masashi Mukae, Himeji, JP;

Yasutaka Takemoto, Himeji, JP;

Toyofumi Sakai, Himeji, JP;

Assignee:
Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C 51/43 (2006.01); B01D 9/00 (2006.01);
U.S. Cl.
CPC ...
C07C 51/43 (2013.01); B01D 9/0045 (2013.01); B01D 9/0059 (2013.01); B01D 2009/0086 (2013.01);
Abstract

The present invention provides a method capable of sufficiently reducing impurities with excellent separation efficiency even from a crystal-containing slurry that contains a low-purity mother liquor and has poor solid-liquid separation properties. The present invention relates to a method for producing a compound, the method including: a step of feeding a slurry containing crystals of the compound to a hydraulic wash column; a step of melting crystals in a crystal-containing circulation slurry discharged from the hydraulic wash column; and a step of returning a portion of a circulation liquid containing a melt obtained in the melting step to the hydraulic wash column, wherein the circulation liquid returned in the returning step in an amount of more than 30% by mass relative to 100% by mass of the melt serves as a washing liquid for crystals.


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