The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Sep. 30, 2025

Filed:

May. 20, 2025
Applicants:

Nagaoka University of Technology, Nagaoka, JP;

Altech Co., Ltd., Tokyo, JP;

Inventors:

Motohiro Tagaya, Nagaoka, JP;

Yanni Zhou, Nagaoka, JP;

Zizhen Liu, Nagaoka, JP;

Yoshinori Matsuura, Saitama, JP;

Isamu Arakawa, Tokyo, JP;

Assignees:
Attorneys:
Primary Examiner:
Int. Cl.
CPC ...
C30B 29/14 (2006.01); C25D 13/02 (2006.01); C25D 13/12 (2006.01); C30B 7/12 (2006.01); C30B 29/68 (2006.01); C30B 33/00 (2006.01); G01N 29/02 (2006.01);
U.S. Cl.
CPC ...
C30B 29/14 (2013.01); C25D 13/02 (2013.01); C25D 13/12 (2013.01); C30B 7/12 (2013.01); C30B 29/68 (2013.01); C30B 33/00 (2013.01); G01N 29/022 (2013.01);
Abstract

Electrophoresis of an ethanol dispersion of an octacalcium phosphate (OCP) crystal is performed to form a multilayer deposited film of the OCP crystal on a cathode (gold sensor) that is an electrode made of a conductive material such as gold. The multilayer deposited film is subjected to ultrasonic cleaning to form a single-layer deposited film of the OCP crystal on the cathode. The OCP crystalline film formed on the gold sensor surface is a stable crystalline film having a layered structure in which a hydrated layer and an apatite layer are regularly repeated, where a specific crystal plane is oriented in a specific direction with the hydrated layer being an uppermost layer.


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