The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jun. 24, 2025

Filed:

Mar. 26, 2021
Applicant:

University of New Hampshire, Durham, NH (US);

Inventors:

David S. Lashmore, Lebanon, NH (US);

Tyler Bennett, Durham, NH (US);

Assignee:

University of New Hampshire, Durham, NH (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
B01J 23/745 (2006.01); B01J 35/00 (2024.01); B01J 35/02 (2006.01); B01J 35/23 (2024.01); B01J 35/30 (2024.01); B01J 35/40 (2024.01); B01J 37/02 (2006.01); B01J 37/16 (2006.01); C01B 21/064 (2006.01); C01B 32/162 (2017.01); C23C 16/26 (2006.01); B82Y 40/00 (2011.01);
U.S. Cl.
CPC ...
B01J 23/745 (2013.01); B01J 35/23 (2024.01); B01J 35/30 (2024.01); B01J 35/393 (2024.01); B01J 35/40 (2024.01); B01J 37/0221 (2013.01); B01J 37/16 (2013.01); C01B 21/064 (2013.01); C01B 32/162 (2017.08); C23C 16/26 (2013.01); B82Y 40/00 (2013.01); Y10S 977/742 (2013.01); Y10S 977/843 (2013.01); Y10S 977/891 (2013.01);
Abstract

Techniques and methods are disclosed for producing a plurality of nanoparticles that can be used as catalysts to grow carbon or boron nitride nanotubes. The method includes mixing an iron salt including a ferrous or ferric ion with a long chain amine, thiol or polyphenol in a solvent comprising alcohol to produce a solution. Ferric or ferrous ion is reduced to zero valence iron. Nucleation of iron nanoparticles is initialized. The iron nanoparticles are capped to retard nanoparticle growth. The nanoparticles include an elemental iron core coated with a polyphenol that isolates the core from oxygen. The nanoparticles include an average diameter of less than or equal to 15.8 nanometers. The iron core may further include a secondary metal to form an iron-alloy. The secondary metal, in some applications, can be a transition metal.


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