Silicon-based solid amine sorbent for coand making method thereof

Abstract

A silicon-based solid amine sorbent for COand the making method thereof including: providing a silicon source liquid which is a silicate solution or a liquid organosilicate, wherein the silicate solution comprises water and a first silicate dissolved in the water; mixing the silicon source liquid with a precipitant to perform a precipitation reaction to obtain a product liquid containing a precipitate, wherein the precipitate is a second silicate or silicic acid; filtering out the precipitate and washing the precipitate with water; mixing the precipitate filtrated out but not dried yet with an organic alcohol and then performing an azeotropic distillation to obtain a dehydrated precipitate; calcining the dehydrated precipitate to obtain a silicon-based support, wherein the silicon-based support is a powder of the second silicate powder or a silica powder; and impregnating the silicon-based support with an organic amine solution and then drying to obtain the silicon-based amine-containing solid sorbent for CO.