The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Apr. 08, 2025

Filed:

Dec. 17, 2019
Applicant:

Virginia Tech Intellectual Properties, Inc., Blacksburg, VA (US);

Inventors:

Roop L. Mahajan, Fairfax, VA (US);

Seul-Yi Lee, Blacksburg, VA (US);

Assignee:
Attorneys:
Primary Examiner:
Int. Cl.
CPC ...
C01B 32/198 (2017.01); B01J 19/14 (2006.01); C01B 32/194 (2017.01); C01B 32/196 (2017.01);
U.S. Cl.
CPC ...
C01B 32/198 (2017.08); B01J 19/14 (2013.01); C01B 32/194 (2017.08); C01B 32/196 (2017.08); C01P 2002/85 (2013.01); C01P 2004/03 (2013.01); C01P 2004/04 (2013.01); C01P 2004/61 (2013.01); C01P 2004/62 (2013.01); C01P 2004/64 (2013.01);
Abstract

Methods of making graphene oxide and reduced graphene oxide are provided. The methods can include a simple one-pot synthesis of graphene oxide from a purified coal powder using a mild oxidizing acid. The methods provide for an improved, more cost-effective, and simpler process than conventional methods such as Hummers methods. In some aspects, placing the purified coal powder in the mild oxidation atmosphere includes contacting the purified coal powder with a mild oxidizing acid such as nitric acid, nitrous acid, sulfuric acid, phosphoric acid, benzoic acid, or a combination thereof. In some aspects, the mild oxidizing acid consists essentially of nitric acid. Graphene oxides and reduced graphene oxides prepared by the methods are also provided.


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