The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Mar. 25, 2025

Filed:

Mar. 09, 2020
Applicants:

Veolia Water Solutions & Technologies Support, Saint-Maurice, FR;

Bernard Roy Mack, Natick, MA (US);

Inventor:

Bernard Roy Mack, Natick, MA (US);

Assignee:
Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C01D 15/08 (2006.01); B01D 9/00 (2006.01); B01D 15/36 (2006.01); B01D 61/02 (2006.01); B01D 61/42 (2006.01); B01D 61/44 (2006.01); B01D 61/58 (2006.01); B01J 47/12 (2017.01); C02F 9/00 (2023.01); C02F 1/04 (2023.01); C02F 1/42 (2023.01); C02F 1/44 (2023.01); C02F 1/469 (2023.01); C02F 1/52 (2023.01);
U.S. Cl.
CPC ...
C01D 15/08 (2013.01); B01D 9/0031 (2013.01); B01D 15/362 (2013.01); B01D 61/025 (2013.01); B01D 61/027 (2013.01); B01D 61/029 (2022.08); B01D 61/422 (2013.01); B01D 61/44 (2013.01); B01D 61/58 (2013.01); B01J 47/12 (2013.01); C02F 9/00 (2013.01); B01D 2009/0086 (2013.01); B01D 2311/06 (2013.01); B01D 2311/08 (2013.01); B01D 2311/2512 (2022.08); B01D 2311/2523 (2022.08); B01D 2311/2623 (2013.01); B01D 2311/2642 (2013.01); B01D 2311/2673 (2013.01); C02F 1/04 (2013.01); C02F 1/42 (2013.01); C02F 2001/425 (2013.01); C02F 1/441 (2013.01); C02F 1/442 (2013.01); C02F 1/4693 (2013.01); C02F 1/52 (2013.01); C02F 2001/5218 (2013.01);
Abstract

A method is disclosed for concentrating and purifying an eluate brine and producing a purified lithium compound. An extraction eluate, rich in lithium, is directed to a nanofiltration unit or a softening process that removes sulfate and/or calcium and magnesium. Permeate from the nanofiltration unit or the effluent from the softening process is directed through an electrodialysis unit. As the lithium-rich solution moves through the electrodialysis unit, lithium, sodium and chloride ions pass from the solution through a cation-transfer membrane and an anion-transfer membrane to concentrate compartments. A dilute stream is directed through the concentrate compartments and collects the lithium, sodium and chloride ions. The electrodialysis unit also produces a product stream which contains non-ionized impurities, such as silica and/or boron. Concentrate from the electrodialysis unit is subject to a precipitation process that produces a lithium compound that is subsequently subjected to a purification process.


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