The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Feb. 18, 2025

Filed:

Mar. 24, 2023
Applicants:

Vinegar Technologies Llc, Bellaire, TX (US);

William Marsh Rice University, Houston, TX (US);

Inventors:

Philip M. Singer, Richmond, TX (US);

Yunke Liu, Houston, TX (US);

Xinglin Wang, Houston, TX (US);

George J. Hirasaki, Bellaire, TX (US);

Harold J. Vinegar, West Lake Hills, TX (US);

Assignee:

Vinegar Technologies LLC, West Lake Hills, TX (US);

Attorneys:
Primary Examiner:
Int. Cl.
CPC ...
G01N 24/08 (2006.01); G01R 33/50 (2006.01); G01V 3/32 (2006.01);
U.S. Cl.
CPC ...
G01N 24/081 (2013.01); G01R 33/50 (2013.01); G01V 3/32 (2013.01);
Abstract

A method for separating liquid-like (T) from solid-like (T)H NMR transverse relaxation times in porous media uses novel pulse sequences together with aH NMR spectrometer optimized for geological core samples. The method is applied to obtain 1D Tdistributions and 2D T-Tmaps in organic-rich chalks for quantification of liquid-like signal (micropore fluids, meso-macropore fluids, fluids dissolved in organic matter, and clay-bound water) and solid-like signal (kerogen, bitumen, and clay hydroxyls). The novel pulse sequences comprise a solid-echo, which detects more solid-like signal than an FID. The method is used for fluid typing in micro/meso-macro pores, clay mineral identification, determination of kerogen content, and quantification of solvent-extracted bitumen versus bitumen expelled from kerogen due to swelling from dissolved hydrocarbons. The method is used to quantify the asphaltene, resin, aromatic, and/or saturate content of bitumen in the rock.


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