The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.
The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.
Patent No.:
Date of Patent:
Feb. 04, 2025
Filed:
Feb. 08, 2022
Chinese Academy of Inspection and Quarantine, Beijing, CN;
Qiang Ma, Beijing, CN;
Chinese Academy of Inspection and Quarantine, Beijing, CN;
Abstract
The invention discloses a detection method based on supercritical fluid chromatography (SFC) and post-column dicationic ionic liquid (DIL) charge complexation, which includes the following steps: (1) The supramolecular solvent (SUPRAS) was prepared by mixing heptanol, tetrahydrofuran, and water; (2) Sample pretreatment: the SUPRAS was used to extract the sample for subsequent analysis; (3) Analysis of perfluorinated compounds (PFCs) using SFC separation, post-column DIL-based charge complexation, and electrospray ionization-mass spectrometry (ESI-MS). The invention established a novel analytical method for the detection of PFCs in textiles incorporating post-chromatographic DIL-based charge complexation and SFC coupled with ESI-MS. The DIL reagent formed positively charged complexes with anionic analytes during the ESI process, facilitating MS detection in the positive ion mode with enhanced detection sensitivity.