The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Dec. 31, 2024

Filed:

Apr. 14, 2020
Applicants:

Covestro Deutschland Ag, Leverkusen, DE;

Covestro Intellectual Property Gmbh & Co. KG, Leverkusen, DE;

Inventors:

Thomas Knauf, Dormagen, DE;

Murat Kalem, Neuss, DE;

Christian Drumm, Frohnhofen, DE;

Alexandre Racoes, Krefeld, DE;

Assignee:

Covestro Deutschland AG, Leverkusen, DE;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C 201/08 (2006.01); B01D 17/02 (2006.01); B01D 19/00 (2006.01); B01J 19/24 (2006.01); C07C 201/16 (2006.01);
U.S. Cl.
CPC ...
C07C 201/08 (2013.01); B01D 17/02 (2013.01); B01D 19/0057 (2013.01); B01J 19/2425 (2013.01); C07C 201/16 (2013.01); B01J 2219/00033 (2013.01);
Abstract

The invention relates to a continuously operating process for producing nitrobenzene, comprising the following steps: a) nitriding benzene in adiabatic conditions with sulfuric acid and nitric acid, using a stoichiometric excess of benzene in relation to the nitric acid; b) first separating a gaseous phase containing benzene and gaseous secondary components from the raw process product of the nitridation in a gas separator provided specifically for this purpose, then separating, in a downstream phase-separating apparatus, the resulting liquid phase, which is depleted in gaseous components and contains nitrobenzene and sulfuric acid, into a sulfuric acid phase and a nitrobenzene phase; and c) processing the nitrobenzene phase, obtaining nitrobenzene. The invention also relates to a production plant suitable for carrying out the claimed process.


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