The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Sep. 24, 2024

Filed:

Dec. 20, 2022
Applicant:

Saudi Arabian Oil Company, Dhahran, SA;

Inventor:

Ke Zhang, Stoneham, MA (US);

Assignee:
Attorney:
Primary Examiner:
Int. Cl.
CPC ...
B01J 29/70 (2006.01); B01J 35/10 (2006.01); B01J 35/61 (2024.01); B01J 35/63 (2024.01); B01J 35/64 (2024.01); B01J 37/04 (2006.01); B01J 37/30 (2006.01); C01B 39/02 (2006.01); C01B 39/46 (2006.01);
U.S. Cl.
CPC ...
B01J 29/7007 (2013.01); B01J 35/617 (2024.01); B01J 35/633 (2024.01); B01J 35/647 (2024.01); B01J 37/04 (2013.01); B01J 37/30 (2013.01); C01B 39/026 (2013.01); C01B 39/46 (2013.01); B01J 2229/14 (2013.01); B01J 2229/37 (2013.01); B01J 2229/38 (2013.01); C01P 2006/12 (2013.01); C01P 2006/14 (2013.01); C01P 2006/16 (2013.01);
Abstract

A method for producing a hierarchical mesoporous beta includes mixing a beta zeolite with an aqueous metal hydroxide solution and heating the beta zeolite and the aqueous metal hydroxide mixture to produce a desilicated beta zeolite, contacting the desilicated beta zeolite with an ammonium salt solution to produce an intermediate hierarchical mesoporous beta zeolite, and treating the intermediate hierarchical mesoporous beta zeolite with an acidic solution to produce the hierarchical mesoporous beta zeolite. The hierarchical mesoporous beta zeolite includes a molar ratio of silicon to aluminum of greater than 12.5, a total pore volume of greater than or equal to the total pore volume of the intermediate hierarchical mesoporous beta zeolite, and an average mesopore size of greater than or equal to the average mesopore size of the hierarchical mesoporous beta zeolite. The method may also include calcining the intermediate hierarchical mesoporous beta zeolite.


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