The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Sep. 10, 2024

Filed:

Feb. 19, 2024
Applicant:

King Faisal University, Al-Ahsa, SA;

Inventors:

Saad Shaaban, Al-Ahsa, SA;

Manal Amin Hessien, Liverpool, GB;

Amr Negm, Liverpool, GB;

Tarek A. Yousef, Al-Ahsa, SA;

Assignee:

KING FAISAL UNIVERSITY, Al-Ahsa, SA;

Attorneys:
Primary Examiner:
Int. Cl.
CPC ...
C08F 289/00 (2006.01); B01D 67/00 (2006.01); B01D 71/10 (2006.01); B01D 71/82 (2006.01); C02F 1/44 (2023.01); C02F 101/30 (2006.01); C08H 8/00 (2010.01); C08J 5/18 (2006.01);
U.S. Cl.
CPC ...
C08F 289/00 (2013.01); B01D 67/0011 (2013.01); B01D 67/0013 (2013.01); B01D 71/10 (2013.01); B01D 71/82 (2013.01); C02F 1/44 (2013.01); C08H 8/00 (2013.01); C08J 5/18 (2013.01); B01D 2323/08 (2013.01); B01D 2323/42 (2013.01); C02F 2101/301 (2013.01); C08J 2351/08 (2013.01);
Abstract

A method of making a lignocellulose incorporating methacrylate functionality from date palm biomass can include extracting sieved date palm biomass at a first predetermined temperature (110° C.) to obtain an extracted date palm biomass; adding an acid to the extracted date palm biomass to obtain a mixture and stirring and refluxing the mixture at a second predetermined temperature (100° C.) to obtain a refluxed cellulose-hemicellulose-lignin residue; dissolving the refluxed cellulose-hemicellulose-lignin residue in a solvent to obtain a solution; adding triethylamine and methacrylic anhydride to the solution to obtain a reaction solution mixture and stirring while heating the reaction solution mixture to react the triethylamine and the methacrylic anhydride with the solution to obtain a reacted solution mixture; pouring the reacted solution mixture into an ice-cold solvent to obtain a solution mixture and separating cellulose-hemicellulose-lignin residue from the solution mixture via centrifuging; dissolving centrifuged cellulose-lignin residue in water to obtain the lignocellulose incorporating methacrylate functionality.


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