The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Sep. 03, 2024

Filed:

Mar. 21, 2022
Applicant:

Waters Technologies Corporation, Milford, MA (US);

Inventor:

Fabrice Gritti, Franklin, MA (US);

Assignee:
Attorneys:
Primary Examiner:
Int. Cl.
CPC ...
G01N 30/46 (2006.01); G01N 30/02 (2006.01); G01N 30/32 (2006.01); G01N 30/82 (2006.01); G01N 30/30 (2006.01);
U.S. Cl.
CPC ...
G01N 30/461 (2013.01); G01N 30/82 (2013.01); G01N 2030/027 (2013.01); G01N 2030/3007 (2013.01); G01N 2030/326 (2013.01); G01N 2030/328 (2013.01);
Abstract

The disclosure relates to a gradient twin column recycling chromatography method that is used to separate a mixture containing closely eluting compounds. In one embodiment, a sample includes a primary organic compound and one or more impurities that closely elute with the primary organic compound. A gradient mobile phase is initially used to remove unwanted early eluting and late eluting impurities from the sample. After the gradient removal of some of the impurities is complete, the remaining mixture of the primary organic compound and the closely eluting impurities are separated using recycle chromatography methodology with an isocratic mobile phase.


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