The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Aug. 06, 2024

Filed:

Sep. 30, 2020
Applicant:

Government of the United States, As Represented BY the Secretary of the Air Force, Wright-Patterson AFB, OH (US);

Inventors:

Ali M. Jawaid, Fairborn, OH (US);

Richard A. Vaia, Beavercreek, OH (US);

Asra Hassan, Tallahassee, FL (US);

Attorneys:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
C04B 35/56 (2006.01); C01B 21/06 (2006.01); C01B 32/90 (2017.01); C04B 35/622 (2006.01); C04B 41/00 (2006.01); C04B 41/53 (2006.01);
U.S. Cl.
CPC ...
C04B 35/5611 (2013.01); C01B 21/0602 (2013.01); C01B 32/90 (2017.08); C04B 35/622 (2013.01); C04B 41/009 (2013.01); C04B 41/5338 (2013.01); C01P 2002/20 (2013.01); C04B 2235/3817 (2013.01); C04B 2235/444 (2013.01); C04B 2235/74 (2013.01);
Abstract

A method of making a layered MXene material comprises a) introducing dried MAX phase powder into a vessel under anhydrous, inert conditions, the MAX phase powder comprising a general formula of M+1AX(n=1, 2, 3, or 4), wherein M is a transition metal or p-block metalloid selected from the group consisting of Ti, Zr, Hf, V, Nb, Ta, Cr, Mo, W, Re, Cu, Ni, Ag, Zn, Cd, In, Sn, and Pb; interlayer A is a Group III, IV, or V metalloid selected from the group consisting of Al, Si, Ga, Ge, In, Sn, Pb, As, Bi, Sb, and X is one of C (carbon) and N (nitrogen); b) introducing a halogen and solvent to the dried MAX phase to create a halogen solution having a predetermined concentration; c) allowing a reaction to proceed for about 24 hours between 30-90° C. to create a reaction slurry comprising a MXene material.


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