The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jul. 16, 2024

Filed:

Oct. 18, 2023
Applicant:

King Saud University, Riyadh, SA;

Inventors:
Assignee:

KING SAUD UNIVERSITY, Riyadh, SA;

Attorneys:
Primary Examiner:
Int. Cl.
CPC ...
C07C 7/135 (2006.01); B01D 53/02 (2006.01); B01J 20/10 (2006.01); B01J 20/26 (2006.01); B01J 20/28 (2006.01);
U.S. Cl.
CPC ...
C07C 7/135 (2013.01); B01D 53/025 (2013.01); B01J 20/103 (2013.01); B01J 20/262 (2013.01); B01J 20/28052 (2013.01); B01D 2253/202 (2013.01); B01D 2253/25 (2013.01); B01D 2256/24 (2013.01); B01D 2257/70 (2013.01); B01D 2257/7022 (2013.01); B01D 2257/7027 (2013.01); B01J 2220/46 (2013.01); B01J 2220/86 (2013.01);
Abstract

The method of making a wall-coated open tubular capillary column with a poly benzyl stationary phase is a method of preparing a capillary column for gas chromatography. An inner wall of a fused silica capillary column is cleaned and then rinsed with a sodium hydroxide solution. The fused silica capillary column is flushed with isopropanol to form a pre-treated capillary column, and the pre-treated capillary column is loaded with a mixture of phenyl tri-methoxy silane and alcohol. The loaded pre-treated capillary column is heated to form a treated capillary column, which is then washed. A thin layer of a poly benzyl stationary phase is then coated on the inner wall through condensation polymerization of benzyl chloride monomers with a Lewis acid catalyst in a non-polar solvent.


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