The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jul. 16, 2024

Filed:

Jan. 15, 2020
Applicant:

Dow Global Technologies Llc, Midland, MI (US);

Inventors:

Junqiang Liu, Freeport, TX (US);

Liren Xu, Spring, TX (US);

Janet M. Goss, Saginaw, MI (US);

Troy D. Wolford, Midland, MI (US);

Assignee:

Dow Global Technologies LLC, Midland, MI (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
B01D 67/00 (2006.01); B01D 53/22 (2006.01); B01D 69/02 (2006.01); B01D 69/08 (2006.01); B01D 71/02 (2006.01); B01D 71/30 (2006.01); B01D 71/64 (2006.01); B01D 71/76 (2006.01); B29D 99/00 (2010.01); B29K 105/00 (2006.01);
U.S. Cl.
CPC ...
B01D 71/301 (2022.08); B01D 53/228 (2013.01); B01D 67/0083 (2013.01); B01D 69/02 (2013.01); B01D 69/08 (2013.01); B01D 71/021 (2013.01); B01D 71/643 (2022.08); B01D 71/76 (2013.01); B29D 99/005 (2013.01); B01D 2325/0233 (2022.08); B29K 2105/0085 (2013.01);
Abstract

A carbon molecular sieve (CMS) membrane may advantageously be made by pyrolyzing a membrane precursor composition comprised of a carbon forming polymer (e.g., polyimide) blended with a polyvinylidene chloride copolymer (PVDC), the polyvinylidene chloride copolymer being the reaction product of at least 60% to 97% by weight of vinylidene chloride and at least one other comonomer and the carbon forming polymer to polyvinylidene chloride copolymer has a weight ratio of greater than 1 to 99. The membrane precursor composition may be formed by dissolving the carbon forming polymer and PVDC in a solvent to form a dope solution. The dope solution may be shaped, for example, into an asymmetric hollow fiber. The asymmetric hollow fiber may be heated to a temperature to dehydrochorinate the PVDC and then subsequently heated in a non-oxidizing atmosphere to carbonize the polymers of the shaped membrane to form the CMS membrane.


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