The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jun. 25, 2024

Filed:

Nov. 22, 2021
Applicant:

Board of Trustees of Michigan State University, East Lansing, MI (US);

Inventors:

Muhammad Rabnawaz, East Lansing, MI (US);

Muhammad Naveed, East Lansing, MI (US);

Assignee:
Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C08K 5/14 (2006.01); C08J 3/24 (2006.01); C08J 11/18 (2006.01); C08K 5/00 (2006.01); C08K 5/053 (2006.01); C08K 5/1539 (2006.01); C08K 5/20 (2006.01); C08L 51/06 (2006.01);
U.S. Cl.
CPC ...
C08J 3/243 (2013.01); C08J 11/18 (2013.01); C08K 5/0025 (2013.01); C08K 5/053 (2013.01); C08K 5/14 (2013.01); C08K 5/1539 (2013.01); C08K 5/20 (2013.01); C08L 51/06 (2013.01); C08J 2323/06 (2013.01); C08J 2323/12 (2013.01); C08L 2207/062 (2013.01); C08L 2312/00 (2013.01); C08L 2314/00 (2013.01);
Abstract

The disclosure relates to thermally reversibly crosslinked polyolefins (TRC-PO) and methods for making the same. A TRC-PO can be formed by reactive melt-processing a mixture including (i) a polyolefin, (ii) an initiator, and (iii) a reversible crosslinker. The reversible crosslinker includes (A) a grafting agent moiety selected from unsaturated cyclic anhydrides, unsaturated cyclic imides, cyclic nitroxides, and ring-opened analogs thereof, and (B) a crosslinking moiety bound to the cyclic grafting agent moiety. This reactive melt-processing, for example including reactive extrusion, forms a thermally reversibly crosslinked (TRC) polyolefin with polyolefin chains reversibly crosslinked via the reversible crosslinkers, which provide dynamic covalent bonds, such as siloxanes and esters, that are amenable to melt re-processing to re-from or otherwise re-use the TRC-PO while still retaining the reversible crosslinks after re-processing. Catalysts and additives such as rheology modifiers can be added to the melt-processing mixture.


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