The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jun. 18, 2024

Filed:

Oct. 18, 2021
Applicant:

Kun Shan University, Tainan, TW;

Inventors:

Hao-Lin Hsu, Tainan, TW;

Jean-Hong Chen, Tainan, TW;

Assignee:

KUN SHAN UNIVERSITY, Tainan, TW;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
H01M 4/133 (2010.01); B01J 19/14 (2006.01); B01J 21/08 (2006.01); B01J 23/887 (2006.01); B01J 37/04 (2006.01); B01J 37/08 (2006.01); B01J 37/18 (2006.01); C01B 32/162 (2017.01); C23C 16/26 (2006.01); H01M 4/04 (2006.01);
U.S. Cl.
CPC ...
C01B 32/162 (2017.08); B01J 19/14 (2013.01); B01J 21/08 (2013.01); B01J 23/8872 (2013.01); B01J 37/04 (2013.01); B01J 37/08 (2013.01); B01J 37/18 (2013.01); C23C 16/26 (2013.01); H01M 4/0428 (2013.01); H01M 4/133 (2013.01); C01B 2202/06 (2013.01); C01B 2202/22 (2013.01);
Abstract

3D bundle-shaped multi-walled carbon nanotubes and preparation method, includes the following steps: uniformly mixing bi-component alloy catalyst and transition metal in an inert gas environment in order to obtain a three-component nano-intermetallic alloy catalyst; disposing the intermetallic catalyst on the substrate; allowing hydrogen to flow through the substrate, and heating the substrate to a first temperature, and using the hydrogen to undergo a reduction of the intermetallic catalyst at the first temperature; applying a protective gas and a carbon source gas, heating the substrate to a second temperature, undergoing a reaction at the second temperature to generate the 3D bundle-shaped multi-walled carbon nanotubes, and collecting the 3D bundle-shaped multi-walled carbon nanotubes after annealing; wherein the second temperature is greater than or equal to the first temperature; a working electrode includes conductive drain material, a conductive bonding gent and a plurality of 3D bundle-shaped multi-walled carbon nanotubes.


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