The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jun. 18, 2024

Filed:

Nov. 29, 2022
Applicant:

Saudi Arabian Oil Company, Dhahran, SA;

Inventors:

Faisal Alotaibi, Al Khobar, SA;

Lianhui Ding, Dhahran, SA;

Assignee:
Attorney:
Primary Examiner:
Int. Cl.
CPC ...
B01J 29/08 (2006.01); B01J 35/23 (2024.01); B01J 35/50 (2024.01); B01J 35/61 (2024.01); B01J 35/63 (2024.01); B01J 35/64 (2024.01); B01J 37/00 (2006.01); B01J 37/03 (2006.01); B01J 37/04 (2006.01); B01J 37/06 (2006.01); B01J 37/08 (2006.01); B01J 37/30 (2006.01); C01B 39/08 (2006.01); C01B 39/24 (2006.01);
U.S. Cl.
CPC ...
B01J 29/084 (2013.01); B01J 35/23 (2024.01); B01J 35/50 (2024.01); B01J 35/617 (2024.01); B01J 35/633 (2024.01); B01J 35/635 (2024.01); B01J 35/647 (2024.01); B01J 37/009 (2013.01); B01J 37/036 (2013.01); B01J 37/04 (2013.01); B01J 37/06 (2013.01); B01J 37/08 (2013.01); B01J 37/30 (2013.01); C01B 39/08 (2013.01); C01B 39/24 (2013.01); B01J 2229/16 (2013.01); B01J 2229/32 (2013.01); C01P 2004/03 (2013.01); C01P 2004/62 (2013.01); C01P 2004/64 (2013.01); C01P 2006/12 (2013.01); C01P 2006/14 (2013.01); C01P 2006/16 (2013.01);
Abstract

Methods for synthesizing a mesoporous nano-sized ultra-stable Y zeolite include adding sodium aluminate and colloidal silica to an aqueous NaOH solution and mixing to form a hydrogel having a molar ratio composition of 8 to 12 NaO:AlO:14 SiO:200 to 400 HO. The method further includes heating the hydrogel to an autoclave to form a zeolite precursor which is filtered and washed to form a nano-sized Y zeolite. Further the method includes combining the nano-sized Y zeolite with water to form a nano-sized Y zeolite slurry mixture and then adding a 0.1 to 2.0 M aqueous solution of ammonium hexafluorosilicate to form a dealuminated solution. Finally the method includes filtering and washing the dealuminated solution with water to form an ultra-stable Y zeolite precursor, drying the ultra-stable Y zeolite precursor, and calcining the dried zeolite precursor to form the nano-sized ultra-stable Y zeolite.


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