The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
May. 28, 2024

Filed:

Jul. 02, 2019
Applicant:

Asymchem Laboratories (Tianjin) Co., Ltd., Tianjin, CN;

Inventors:

Hao Hong, Morrisville, NC (US);

Jiangping Lu, Tianjin, CN;

Xichun Feng, Tianjin, CN;

Xingfang Sun, Tianjin, CN;

Feng Zhang, Tianjin, CN;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C 2/86 (2006.01); C07B 37/02 (2006.01);
U.S. Cl.
CPC ...
C07C 2/86 (2013.01); C07B 37/02 (2013.01); C07C 2601/02 (2017.05);
Abstract

The present disclosure discloses a method and a device for continuously synthesizing cyclopropane compounds. The method includes the following steps: continuously performing a synthetic reaction of a diazomethane precursor in a first reactor, the reaction product of the first reactor flowing into a separator for stratification, the organic phase obtained by stratification overflowing into a second reactor, continuously consuming the diazomethane precursor in a second reactor to prepare diazomethane and performing an electron-rich monoolefin cyclopropanation reaction in situ so as to obtain the cyclopropane compound.


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