The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Mar. 26, 2024

Filed:

Nov. 18, 2022
Applicant:

Central South University, Changsha, CN;

Inventors:

Zhang Lin, Changsha, CN;

Xu Yan, Changsha, CN;

Xueming Liu, Changsha, CN;

Fandongkun Meng, Changsha, CN;

Yanjie Liang, Changsha, CN;

Assignee:

Central South University, Changsha, CN;

Attorney:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
C01G 3/10 (2006.01); C02F 1/52 (2023.01); C02F 1/66 (2023.01); C02F 1/72 (2023.01); C02F 9/00 (2023.01); C02F 101/10 (2006.01);
U.S. Cl.
CPC ...
C01G 3/10 (2013.01); C02F 9/00 (2013.01); C01P 2004/03 (2013.01); C02F 1/5236 (2013.01); C02F 1/66 (2013.01); C02F 1/722 (2013.01); C02F 2101/10 (2013.01);
Abstract

The present invention provides a method for treating a copper-containing waste etching solution, which includes: preparing basic copper chloride nanometer seed crystals and synthesizing basic copper chloride mono-crystals; making an acidic waste etching solution subjected to agglomeration reaction with an ammonium-containing solution and slurry containing the basic copper chloride mono-crystals to obtain basic copper chloride crystal particles and copper-removed waste solution; making an alkaline waste etching solution react with sulfuric acid to obtain a copper sulfate mixed solution; and then evaporating, concentrating, cooling and crystallizing the copper sulfate mixed solution obtained by the reaction of the alkaline waste etching solution and the sulfuric acid in sequence to obtain copper sulfate pentahydrate solids. In a case of low investment, the present invention not only can realize the recycling of copper in the copper-containing waste etching solution, but also can obtain various high-value products, and can achieve both environmental and economic benefits.


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