The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jan. 30, 2024

Filed:

Sep. 03, 2019
Applicant:

Basf SE, Ludwigshafen am Rhein, DE;

Inventors:

Oliver Bey, Ludwigshafen am Rhein, DE;

Peter Zehner, Weisenheim am Berg, DE;

Michael Acker, Ludwigshafen am Rhein, DE;

Rocco Paciello, Ludwigshafen am Rhein, DE;

Mathias Schelwies, Ludwigshafen am Rhein, DE;

Martin Haubner, Ludwigshafen am Rhein, DE;

Guenter Wegner, Ludwigshafen am Rhein, DE;

Gerd Tebben, Ludwigshafen am Rhein, DE;

Gunnar Heydrich, Ludwigshafen am Rhein, DE;

Georg Seeber, Ludwigshafen am Rhein, DE;

Assignee:

BASF SE, Ludwigshafen am Rhein, DE;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C 29/141 (2006.01); B01J 10/00 (2006.01); B01J 3/04 (2006.01); B01J 19/00 (2006.01); B01J 19/24 (2006.01); B01J 19/26 (2006.01); B01J 19/30 (2006.01); B01J 19/32 (2006.01); B01J 31/20 (2006.01);
U.S. Cl.
CPC ...
C07C 29/141 (2013.01); B01J 3/042 (2013.01); B01J 10/00 (2013.01); B01J 10/002 (2013.01); B01J 19/0066 (2013.01); B01J 19/244 (2013.01); B01J 19/2465 (2013.01); B01J 19/26 (2013.01); B01J 19/30 (2013.01); B01J 19/32 (2013.01); B01J 31/20 (2013.01); B01J 2219/0009 (2013.01); B01J 2219/0025 (2013.01); B01J 2219/00092 (2013.01); B01J 2219/00096 (2013.01); B01J 2219/185 (2013.01); B01J 2219/1943 (2013.01); B01J 2531/822 (2013.01); C07B 2200/07 (2013.01);
Abstract

A reactor for performing a gas/liquid biphasic high-pressure reaction with a foaming medium, comprising an interior formed by a cylindrical, vertically oriented elongate shell, a bottom and a cap, wherein the interior is divided by internals into a backmixed zone and a zone of limited backmixing, wherein the backmixed zone and the zone of limited backmixing are consecutively traversable by the reaction mixture, wherein the backmixed zone comprises means for introducing gas and liquid and a gas outlet and also comprises at least one mixing apparatus selected from a stirrer, a jet nozzle and means for injecting the gas, and the zone of limited backmixing comprises a reaction product outlet, a first cylindrical internal element which in the interior extends in the longitudinal direction of the reactor and which delimits the zone of limited backmixing from the backmixed zone, backmixing-preventing second internal elements in the form of random packings, structured packings or liquid-permeable trays arranged in the zone of limited backmixing and a riser tube whose lower end is arranged within the backmixed zone and whose upper end opens into the zone of limited backmixing so that liquid from the backmixed zone can ascend into the zone of limited backmixing via the riser tube, wherein flow into the zone of limited backmixing enters from below. The reactor is configured such that the high-pressure reaction space is optimally utilized and contamination of workup steps or subsequent reactions arranged downstream of the high-pressure reaction with foam is substantially avoided. The invention further relates to a process for performing a continuous gas/liquid biphasic high-pressure reaction in the reactor.


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