The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jan. 16, 2024

Filed:

Jul. 05, 2023
Applicant:

Shanghai Wokai Biotechnology Co., Ltd., Shanghai, CN;

Inventors:

Fang Ling, Shanghai, CN;

Ruming Feng, Shanghai, CN;

Yong Feng, Shanghai, CN;

Haiquan Ding, Shanghai, CN;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07D 307/68 (2006.01);
U.S. Cl.
CPC ...
C07D 307/68 (2013.01);
Abstract

A method for preparing FDCA with furfural as a raw material includes (1) pretreatment of the furfural: subjecting the furfural and an alcohol compound to an acetalization reaction under catalysis of an acidic ion resin to obtain an acetal compound of the furfural with the alcohol compound; (2) under stirring, adding the acetal compound dropwise to a mixed liquid of an acylation reagent and an ionic liquid (IL) to allow a reaction for 1 h to 2 h, adding a catalyst to continue the reaction for 3 h to 5 h, and subjecting a resulting reaction system to a post-treatment to obtain 5-acylfurfural; and (3) mixing the 5-acylfurfural with hydrogen peroxide, adding a catalyst to allow an oxidation reaction, and after the oxidation reaction is completed, subjecting a product to washing and recrystallization to obtain a white crystal, which is the FDCA.


Find Patent Forward Citations

Ling, Fang. (2024). Method for preparing 2,5-furandicarboxylic acid (fdca) from furfural (U.S. Patent No. 11873286). U.S. Patent and Trademark Office. https://idiyas.com/patent/badge/11873286

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