The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.
The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.
Patent No.:
Date of Patent:
Jan. 16, 2024
Filed:
Apr. 22, 2016
Applicant:
Ocp SA, Casablanca, MA;
Inventors:
Kamal Samrane, Casablanca, MA;
Abdelaali Kossir, El Jadida, MA;
Assignee:
Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C01F 11/22 (2006.01); C01B 33/18 (2006.01); C01C 1/02 (2006.01); C01C 1/26 (2006.01); B01J 10/00 (2006.01);
U.S. Cl.
CPC ...
C01F 11/22 (2013.01); B01J 10/00 (2013.01); C01B 33/186 (2013.01); C01C 1/026 (2013.01); C01C 1/26 (2013.01); C01P 2004/61 (2013.01); C01P 2006/12 (2013.01); C01P 2006/80 (2013.01);
Abstract
A process for preparing synthetic calcium fluoride (CaF) (min 90% CaFby weight) from fluosilicic acid is provided. The processes comprises the steps of (a) reacting fluosilicic acid (HSiF) with ammonium hydroxide or ammonia in a first reactor so as to obtain a first slurry and filtering the first slurry so as to obtain a filtrate containing a solution of ammonium fluoride (b) precipitating the solution of ammonium fluoride with calcium in a second reactor so as to produce a second slurry containing calcium fluoride and (c) evolving the major part of ammonia from the second reactor and then scrubbing and returning said ammonia to the first reactor.