The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jan. 02, 2024

Filed:

Jan. 15, 2019
Applicant:

Beijing University of Technology, Beijing, CN;

Inventors:

Dean Pan, Beijing, CN;

Yufeng Wu, Beijing, CN;

Assignee:
Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C01B 7/09 (2006.01); C01G 9/06 (2006.01); C01G 21/20 (2006.01); C22B 7/00 (2006.01); C22B 7/02 (2006.01); C22B 3/00 (2006.01);
U.S. Cl.
CPC ...
C01B 7/096 (2013.01); C01G 9/06 (2013.01); C01G 21/20 (2013.01); C22B 7/008 (2013.01); C22B 7/02 (2013.01); C22B 13/045 (2013.01); C22B 19/24 (2013.01);
Abstract

The invention relates to the field of efficient separation and recovery of bromine by full wet method, especially to a two-step separating method of bromide and recovery of lead and zinc from printed circuit board Incineration ash. It mainly includes first sodium hydroxide alkaline leaching, secondary sodium peroxide alkaline leaching, pH adjustment, separate lead and zinc, bromide evaporation and crystallization to recover crude bromide and other steps. Compared with traditional comprehensive recovery process of ash, the invention uses sodium hydroxide to dissolve bromide, lead and zinc, and uses the strong oxidation of sodium peroxide in alkaline environment, copper bromide and other bromine are oxidized and leached; through two-step method, the efficient leaching of bromine, lead and zinc is realized, silver and other precious metals are enriched at the same time. It is beneficial to subsequent recovery of precious metals and has the characteristics of short tail liquid discharge.


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