The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Nov. 21, 2023

Filed:

Apr. 14, 2023
Applicant:

King Fahd University of Petroleum and Minerals, Dhahran, SA;

Inventors:

Mohammad M. Hossain, Dhahran, SA;

Yahya Gambo, Dhahran, SA;

Mohammed S. Ba-Shammakh, Dhahran, SA;

Akolade Idris Bakare, Dhahran, SA;

Sagir Adamu, Dhahran, SA;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
B01J 23/22 (2006.01); B01J 23/02 (2006.01); B01J 35/00 (2006.01); B01J 35/02 (2006.01); B01J 35/10 (2006.01); B01J 37/04 (2006.01); B01J 37/00 (2006.01); B01J 37/08 (2006.01); C07C 5/48 (2006.01); B01J 21/16 (2006.01); C11D 3/12 (2006.01);
U.S. Cl.
CPC ...
B01J 23/22 (2013.01); B01J 21/16 (2013.01); B01J 23/02 (2013.01); B01J 35/006 (2013.01); B01J 35/0013 (2013.01); B01J 35/026 (2013.01); B01J 35/1014 (2013.01); B01J 35/1019 (2013.01); B01J 35/1038 (2013.01); B01J 35/1042 (2013.01); B01J 35/1061 (2013.01); B01J 37/0036 (2013.01); B01J 37/0045 (2013.01); B01J 37/04 (2013.01); B01J 37/086 (2013.01); C07C 5/48 (2013.01); C11D 3/1253 (2013.01); C07C 2521/10 (2013.01); C07C 2523/22 (2013.01);
Abstract

A method of making an active catalyst composition includes mixing at least one support with a vanadium oxide precursor and grinding thereby at least partially embedding the vanadium oxide precursor particles in different layers and surfaces of the at least one support to form a first precursor; mixing the first precursor and a first solvent to form a first mixture; grinding the first mixture and drying at a temperature of 60 to 105° C.; calcining the first mixture after the drying at a temperature of at least 300° C. thereby allowing the vanadium oxide precursor particles embedded in different layers and surfaces of the at least one support to decompose in situ to generate vanadium oxide (VO) particles embedded in the at least one support and form the first vanadium catalyst; and mixing the first vanadium catalyst with a second vanadium catalyst to form the active catalyst composition.


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