The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Oct. 31, 2023

Filed:

Jun. 12, 2020
Applicant:

Nectar Health Sciences Inc., Victoria, CA;

Inventors:

Tony Durst, Ottawa, CA;

Jay Van Der Vlugt, Victoria, CA;

Amanda Saikaley, Ottawa, CA;

Assignee:
Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07D 311/80 (2006.01); C07C 211/63 (2006.01); C07C 215/40 (2006.01); C07D 453/04 (2006.01); C07D 487/04 (2006.01); C07D 487/08 (2006.01); C07C 51/43 (2006.01); C07C 65/19 (2006.01);
U.S. Cl.
CPC ...
C07D 311/80 (2013.01); C07C 51/43 (2013.01); C07C 65/19 (2013.01); C07C 211/63 (2013.01); C07C 215/40 (2013.01); C07D 453/04 (2013.01); C07D 487/04 (2013.01); C07D 487/08 (2013.01);
Abstract

Disclosed are methods for separating, recovering, and purifying cannabidiolic acid (CBDA) salts from an organic solvent solution comprising a mixture of cannabinoids. The methods comprise solubilizing the mixture of cannabinoids in C5-C7 hydrocarbon solvents, adding thereto a selected amine to thereby precipitate a CBDA-amine salt therefrom, dissolving the recovered CBDA-amine salt in a selected solvent and then adding thereto a selected antisolvent to thereby recrystallizing a purified CBDA-amine salt therefrom. The recrystallized CBDA-amine salt may be decarboxylated to form a mixture of cannabidiol (CBD) and amine. The CBD amine mixture may be acidified to separate the amine from CBD. The recovered CBD may be concentrated to produce a highly purified CBD. Also disclosed are CBDA-amine salts produced with certain amines selected from groups of secondary amines, tertiary amines, diamines, amino alcohols, amino ethers, and highly basic amines.


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