The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Oct. 17, 2023

Filed:

May. 19, 2022
Applicant:

Ddp Specialty Electronic Materials Us, Llc, Wilmington, DE (US);

Inventors:

Longyan Liao, Shanghai, CN;

Shari Kram, Midland, MI (US);

Mark Rickard, Midland, MI (US);

Yiyong He, Midland, MI (US);

John Hull, Jr., Midland, MI (US);

Assignee:
Attorney:
Primary Examiner:
Int. Cl.
CPC ...
B01J 31/40 (2006.01); B01J 31/02 (2006.01); B01J 38/42 (2006.01); B01J 38/48 (2006.01); C08F 297/04 (2006.01);
U.S. Cl.
CPC ...
B01J 31/40 (2013.01); B01J 31/0271 (2013.01); B01J 38/42 (2013.01); B01J 38/48 (2013.01); C08F 297/04 (2013.01); B01J 2231/32 (2013.01); B01J 2531/002 (2013.01); C08F 2810/00 (2013.01);
Abstract

Quaternary ammonium tribromides and quaternary phosphonium tribromides are recovered from an organic solvent by washing with an aqueous hydrazine solution. The hydrazine reacts to form nitrogen, hydrobromic acid and a quaternary ammonium or quaternary phosphonium monobromide. The hydrobromic acid and quaternary ammonium or quaternary phosphonium migrate to the aqueous phase, thereby effecting the removal of the tribromides from the organic solvent. The hydrobromic acid can be neutralized with a quaternary ammonium or quaternary phosphonium hydroxide to produce a quaternary ammonium or quaternary phosphonium monobromide. The monobromides produced can be reacted with elemental bromine to regenerate a tribromide brominating agent.


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