The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Sep. 19, 2023

Filed:

Mar. 14, 2019
Applicant:

Tubitak, Ankara, TR;

Inventors:

Iffet Yakar Elbeyli, Kocaeli, TR;

Ahmet Baykan, Istanbul, TR;

Abdullah Zahid Turan, Kocaeli, TR;

Ismail Ersan Kalafatoglu, Istanbul, TR;

Murat Bilen, Ankara, TR;

Erhan Tektas, Ankara, TR;

Fazli Cabbar Metin, Ankara, TR;

Assignee:

TUBITAK, Ankara, TR;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C01B 35/10 (2006.01); B01D 9/00 (2006.01); B01D 15/36 (2006.01); B01D 21/26 (2006.01);
U.S. Cl.
CPC ...
C01B 35/109 (2013.01); B01D 9/0004 (2013.01); B01D 9/0059 (2013.01); B01D 15/362 (2013.01); B01D 15/363 (2013.01); B01D 21/262 (2013.01); B01D 21/267 (2013.01); B01D 2009/0086 (2013.01); C01P 2006/80 (2013.01);
Abstract

The present invention relates to the process of purification of boric acid by ion exchange method. Boric acid is dissolved in hot demineralized water. The hot solution is pressure-filtered. The hot saturated solution, which is purified from water-insoluble, is passed through a column containing strong cation exchange resin, followed by a column containing weak anion exchange resin at the same temperature and cooled afterwards. The crystals settling by cooling are separated from the mother liquor, the amount of aqueous solution within them is reduced and then dried. The waste solution formed during crystallization and filtrate formed after separation of crystals from aqueous solution are mixed and used in boric acid dissolving process. The developed method enables the reduction of sodium, sulfate, chloride and iron impurities of technical grade boric acid to less than 1 ppm and is more economic and environmental friendly than current methods.


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