The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jul. 25, 2023

Filed:

Aug. 19, 2020
Applicant:

Waters Technologies Corporation, Milford, MA (US);

Inventors:

Jason F. Hill, Milford, MA (US);

Martin Gilar, Franklin, MA (US);

Abhijit Tarafder, Blackstone, MA (US);

Christopher DesJardins, Chelmsford, MA (US);

Assignee:
Attorneys:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
G01F 22/02 (2006.01); G01N 30/06 (2006.01); G01N 30/16 (2006.01); G01N 30/02 (2006.01);
U.S. Cl.
CPC ...
G01F 22/02 (2013.01); G01N 30/06 (2013.01); G01N 30/16 (2013.01); G01N 2030/027 (2013.01);
Abstract

Described is a method for determining a dwell volume of a liquid chromatography system and a liquid chromatography system that can determined the system dwell volume. The method includes mixing a flow of a first solvent with a flow of a second solvent to form a solvent mixture. The flows of the first and second solvents are decreased and increased, respectively, to generate a gradient composition. A system pressure of the liquid chromatography system is measured to determine a pressure trace defined as the measured system pressure as a function of time. The dwell volume of the system is determined from a time delay determined between the gradient composition at the mixing location and the pressure trace. The method can be performed with a liquid chromatography system having a chromatographic column or a flow restrictor used in place of the chromatographic column.


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