The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jul. 18, 2023

Filed:

Jun. 02, 2017
Applicant:

Dalian University of Technology, Dalian, CN;

Inventors:

Xie Quan, Dalian, CN;

Gaoliang Wei, Dalian, CN;

Shuo Chen, Dalian, CN;

Hongtao Yu, Dalian, CN;

Assignee:
Attorney:
Primary Examiner:
Int. Cl.
CPC ...
B01D 67/00 (2006.01); B01D 71/02 (2006.01); B01D 69/12 (2006.01); C01B 32/184 (2017.01); B01D 69/02 (2006.01);
U.S. Cl.
CPC ...
B01D 67/0062 (2013.01); B01D 67/0067 (2013.01); B01D 69/02 (2013.01); B01D 69/122 (2013.01); B01D 71/021 (2013.01); C01B 32/184 (2017.08); B01D 67/0011 (2013.01); B01D 2325/04 (2013.01); C01B 2204/02 (2013.01); C01B 2204/04 (2013.01);
Abstract

The invention, belonging to the field of membrane technology, presents a method for the direct growth of ultrathin porous graphene separation membranes. Etching agent, organic solvent and polymer are coated on metal foil, and then they are calcined at high temperature in absence of oxygen; after removal of metal substrate and reaction products, single-layered or multi-layered porous graphene membranes are obtained. Alternatively, the dispersion or solution of etching agent is coated on metal foil, on which a polymer film is then overlaid. The obtained sample is subsequently calcined at high temperature in absence of oxygen; after removal of metal substrate and reaction products, single-layered or multi-layered porous graphene membranes are obtained. The method involved in this invention is simple and highly efficient, and allows direct growth of ultrathin porous graphene separation membranes, without needing expensive apparatuses, chemicals and graphene raw material. Additionally, the graphene membranes prepared with this method have controlled pore size, ultrahigh water flux and strong resistance to irreversible fouling.


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