The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jun. 20, 2023

Filed:

Aug. 20, 2020
Applicant:

Röhm Gmbh, Darmstadt, DE;

Inventors:

Rudolf Burghardt, Darmstadt, DE;

Steffen Krill, Muehltal, DE;

Florian Zschunke, Frankfurt, DE;

Eduard Rundal, Frankfurt, DE;

Torsten Panak, Stockstadt/Rhein, DE;

Daniel Helmut König, Stuttgart, DE;

Assignee:

Röhm GmbH, Darmstadt, DE;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C 45/75 (2006.01); C07C 45/84 (2006.01); B01D 3/14 (2006.01); B01D 5/00 (2006.01); B01D 17/02 (2006.01); B01J 14/00 (2006.01);
U.S. Cl.
CPC ...
C07C 45/75 (2013.01); B01D 3/145 (2013.01); B01D 5/006 (2013.01); B01D 17/0214 (2013.01); B01J 14/005 (2013.01); C07C 45/84 (2013.01);
Abstract

A process and a preparation plant prepares methacrolein from formaldehyde and propionaldehyde, in presence of water and a homogeneous catalyst based at least on an acid and a base. A reaction mixture is introduced into a methacrolein workup plant and separated in a first distillation column, into a first distillation mixture in a gas phase at the top and a second distillation mixture in a liquid phase at the bottom. The first distillation mixture is condensed and, in a first phase separator, the organic phase and the aqueous phase of the condensate are separated from one another. The aqueous phase is introduced into a second distillation column, that is not part of the methacrolein workup plant, and is separated into a third distillation mixture in a gas phase at the top and a fourth distillation mixture at the bottom. The third distillation mixture is introduced into the methacrolein workup plant.


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