The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.
The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.
Patent No.:
Date of Patent:
May. 30, 2023
Filed:
Aug. 04, 2021
The United States of America As Represented BY the Secretary of the Navy, Indian Head, MD (US);
Robert C. Brothers, Potomac, MD (US);
Rebecca Wilson, Alexandria, VA (US);
The United States of America as represented by the Secretary of the Navy, Washington, DC (US);
Abstract
A method of making a polysilylether (PSE) polymer includes: cooling a solution of diethylamine to 0° C. under argon; adding cold dialkyldichlorosilane to form a first mixture; slowly warming the first mixture to form dialkylbis(diethylamino)silane; diluting the first mixture with hexane then filtering via cannula; evaporating the hexane and excess diethylamine; purifying the dialkylbis(diethylamino)silane under vacuum distillation; adding the dialkylbis(diethylamino)silane to a solution of diol dissolved in tetrahydrofuran to form a second mixture; heating the second mixture to 60° C. while reflux condensing, and cooling and concentrating the second mixture under vacuum to form a resultant mixture containing the polysilylether (PSE) polymer.