The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Apr. 04, 2023

Filed:

Mar. 19, 2021
Applicants:

Saudi Arabian Oil Company, Dhahran, SA;

King Fahd University of Petroleum & Minerals, Dhahran, SA;

Inventors:

Emad Al-Shafei, Dhahran, SA;

Oki Muraza, Dhahran, SA;

Anas Karrar Jamil, Al-Khobar, SA;

Ki-Hyouk Choi, Dhahran, SA;

Ashok K. Punetha, Dhahran, SA;

Zain Hassan Yamani, Dhahran, SA;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C01B 39/02 (2006.01); B01J 29/70 (2006.01); B01J 6/00 (2006.01); B01J 19/00 (2006.01); B01J 19/28 (2006.01); B01J 35/02 (2006.01); B01J 37/04 (2006.01); B01J 37/08 (2006.01); C10G 11/05 (2006.01); C01B 39/48 (2006.01); C01B 39/46 (2006.01);
U.S. Cl.
CPC ...
B01J 29/7042 (2013.01); B01J 6/002 (2013.01); B01J 19/0013 (2013.01); B01J 19/28 (2013.01); B01J 35/023 (2013.01); B01J 37/04 (2013.01); B01J 37/08 (2013.01); C01B 39/02 (2013.01); C01B 39/46 (2013.01); C01B 39/48 (2013.01); C10G 11/05 (2013.01); B01J 2219/0009 (2013.01); B01J 2219/00189 (2013.01); C10G 2300/1044 (2013.01); C10G 2300/703 (2013.01); C10G 2400/20 (2013.01); C10G 2400/22 (2013.01);
Abstract

According to one or more embodiments, non-agglomerated, nano-sized ZSM-22 zeolites may be synthesized by methods comprising operating a mechanical rotation drum unit at a first temperature of from 40° C. to 60° C. and a first speed of from 200 rpm to 1000 rpm for a first time period of from 1.3 hours to 2.7 hours; operating the mechanical rotation drum unit at a second speed of from 30 rpm to 90 rpm for a second time period of from 0.05 hours to 0.4 hours; heating the mechanical rotation drum unit at a ramping temperature of from 8° C./minute to 12° C./minute to a second temperature of from 115° C. to 185° C. at the second speed; operating the mechanical rotation drum unit at the second temperature and the second speed for a third time period of from 30 hours to 90 hours; and cooling the mechanical rotation drum unit at a fourth speed of 0 rpm.


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