The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Mar. 28, 2023

Filed:

Nov. 26, 2018
Applicant:

Sulzer Management Ag, Winterthur, CH;

Inventors:

Peter Faessler, Allschwil, CH;

Manfred Stepanski, Buchs, CH;

Halbe Jansen, Eschlikon, CH;

Assignee:

SULZER MANAGEMENT AG, Winterthur, CH;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C 265/14 (2006.01); B01D 3/26 (2006.01); B01D 5/00 (2006.01); B01D 1/22 (2006.01); B01D 9/00 (2006.01); C07C 263/20 (2006.01);
U.S. Cl.
CPC ...
C07C 265/14 (2013.01); B01D 1/22 (2013.01); B01D 3/26 (2013.01); B01D 5/0003 (2013.01); B01D 5/006 (2013.01); B01D 5/009 (2013.01); B01D 9/0013 (2013.01); C07C 263/20 (2013.01); B01D 2009/0086 (2013.01);
Abstract

A plant for preparing a purified isomeric methylene diphenyl diisocyanate monomer from a mixture of different isomeric monomers is disclosed herein. The plant can comprise a distillation apparatus, which comprises: a) a distillation column including a structured packing, b) a source for a mixture of different isomeric methylene diphenyl diisocyanate monomers, c) an evaporator, d) an overhead vapor condenser, e) optionally, an overhead vacuum system and f) a flow-controlled reflux system. The overhead vapor condenser comprises a shell and tube arrangement and is embodied so as to directly subcool the condensate to less than 47° C. The flow-controlled reflux system comprises a heater, which is embodied so as to reheat a partial stream of the condensate formed in the overhead vapor condenser up to 190° C.


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