The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Dec. 27, 2022

Filed:

Aug. 21, 2020
Applicant:

Nanjing Tech University, Nanjing, CN;

Inventors:

Kai Guo, Nanjing, CN;

Zheng Fang, Nanjing, CN;

Man Yang, Nanjing, CN;

Junjie Tao, Nanjing, CN;

Ning Zhu, Nanjing, CN;

Wei He, Nanjing, CN;

Kequan Chen, Nanjing, CN;

Pingkai Ouyang, Nanjing, CN;

Assignee:
Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C08G 71/04 (2006.01); C08G 18/32 (2006.01); C08G 18/76 (2006.01); C08G 18/64 (2006.01); C08G 18/08 (2006.01); C08G 18/48 (2006.01); C08G 18/10 (2006.01); C08G 18/36 (2006.01); C08G 18/18 (2006.01); C08G 18/67 (2006.01); C08G 65/26 (2006.01); C08G 18/20 (2006.01); C08G 18/16 (2006.01); B01J 19/00 (2006.01); C08G 18/24 (2006.01);
U.S. Cl.
CPC ...
C08G 71/04 (2013.01); B01J 19/0093 (2013.01); C08G 18/08 (2013.01); C08G 18/10 (2013.01); C08G 18/165 (2013.01); C08G 18/1833 (2013.01); C08G 18/2081 (2013.01); C08G 18/246 (2013.01); C08G 18/3203 (2013.01); C08G 18/3206 (2013.01); C08G 18/36 (2013.01); C08G 18/4895 (2013.01); C08G 18/6407 (2013.01); C08G 18/6795 (2013.01); C08G 18/7671 (2013.01); C08G 18/7685 (2013.01); C08G 65/2609 (2013.01); B01J 2219/0081 (2013.01); B01J 2219/00781 (2013.01); B01J 2219/00889 (2013.01); B01J 2219/00961 (2013.01); B01J 2219/00984 (2013.01);
Abstract

A method for preparing a polyol comprises the following steps of: (1) dissolving 2,3 -epoxybutane and an acid catalyst in an inert solvent to obtain a solution A; dissolving triethylene glycol in an inert solvent to obtain a solution B; and dissolving epoxy vegetable oil in an inert solvent to obtain a solution C; (2) respectively and simultaneously pumping the solutions A and B into a first micromixer for mixing; (3) pumping the solution C and an effluent of the first microreactor into a second micromixer for mixing while carrying out step (2); and (4) dissolving the vegetable oil polyol in an inert solvent to obtain a solution D; dissolving epoxypropane and an alkaline catalyst in an inert solvent to obtain a solution E; and pumping the solution D and the solution E into a tank reactor for reaction, thereby obtaining the polyol.


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